Publication
Effect of Annealing Heat Treatment on the Composition, Morphology, Structure and Mechanical Properties of the W-S-N Coatings
| dc.contributor.author | Yaqub, Talha Bin | |
| dc.contributor.author | Al-Rjoub, Abbas | |
| dc.contributor.author | Khalid, Hafiza Ayesha | |
| dc.contributor.author | Yaqoob, Khurram | |
| dc.contributor.author | Fernandes, Filipe | |
| dc.contributor.author | Cavaleiro, Albano | |
| dc.date.accessioned | 2023-01-30T15:20:49Z | |
| dc.date.available | 2023-01-30T15:20:49Z | |
| dc.date.issued | 2022 | |
| dc.description.abstract | Alloyed-transition metal dichalcogenide (TMD) coatings have been under investigation as multi-environment lubricants for the past few decades. These coatings display very low coefficient of friction properties at elevated temperatures. Studies on the annealing of these low-friction coatings are missing in the literature. For the first time, in this study, the annealing of the W-S-N dry lubricant coatings was carried out to study its effects on the composition, morphology, crystal structure and hardness of the coatings. The W-S-N coatings were deposited by direct current (DC) reactive magnetron sputtering. The analysis was carried out for as-deposited, 200 °C and 400 °C annealed coatings. The as-deposited coatings have N content in the range of 0–25.5 at. %. The coatings are compact and the densification increased with the increase in N-alloying. All the coatings are crystalline except the highest N-alloyed coating which is X-ray amorphous. A maximum hardness of 8.0 GPa was measured for the coating alloyed with 23 at. % N. Annealing did not affect the composition and morphology of the coatings, while some variations were observed in their crystal structure and hardness. The maximum hardness increased from 8 GPa to 9.2 GPa after 400 °C annealing of the 23 at. % N-alloyed coating. | pt_PT |
| dc.description.sponsorship | This study is sponsored by FEDER National funds FCT under the projects: SMARTLUB ref.“POCI-01-0145-FEDER-031807”, CEMMPRE ref. “UIDB/00285/2020”, On-SURF ref. “POCI-01-0247-FEDER-024521”, “LA/P/0112/2020” and Atrito-0 ref. “POCI-01-0145-FEDER-030446”. | pt_PT |
| dc.description.version | info:eu-repo/semantics/publishedVersion | pt_PT |
| dc.identifier.doi | 10.3390/ma15124088 | pt_PT |
| dc.identifier.uri | http://hdl.handle.net/10400.22/22013 | |
| dc.language.iso | eng | pt_PT |
| dc.publisher | MDPI | pt_PT |
| dc.relation | POCI-01-0145-FEDER-031807 | pt_PT |
| dc.relation | Centre for Mechanical Enginnering, Materials and Processes | |
| dc.relation | LA/P/0112/2020 | pt_PT |
| dc.relation | POCI-01-0145-FEDER-030446 | pt_PT |
| dc.relation.publisherversion | https://www.mdpi.com/1996-1944/15/12/4088 | pt_PT |
| dc.rights.uri | http://creativecommons.org/licenses/by-nc-nd/4.0/ | pt_PT |
| dc.subject | Transition metal dichalcogenides | pt_PT |
| dc.subject | W-S-N coatings | pt_PT |
| dc.subject | Annealing | pt_PT |
| dc.subject | Crystal structure | pt_PT |
| dc.subject | Hardness | pt_PT |
| dc.subject | Dry lubricants | pt_PT |
| dc.title | Effect of Annealing Heat Treatment on the Composition, Morphology, Structure and Mechanical Properties of the W-S-N Coatings | pt_PT |
| dc.type | journal article | |
| dspace.entity.type | Publication | |
| oaire.awardTitle | Centre for Mechanical Enginnering, Materials and Processes | |
| oaire.awardURI | info:eu-repo/grantAgreement/FCT/6817 - DCRRNI ID/UIDB%2F00285%2F2020/PT | |
| oaire.citation.issue | 12 | pt_PT |
| oaire.citation.startPage | 4088 | pt_PT |
| oaire.citation.title | Materials | pt_PT |
| oaire.citation.volume | 15 | pt_PT |
| oaire.fundingStream | 6817 - DCRRNI ID | |
| person.familyName | Fernandes | |
| person.givenName | Filipe | |
| person.identifier | 995468 | |
| person.identifier.ciencia-id | 2113-A18B-EEE8 | |
| person.identifier.orcid | 0000-0003-4035-3241 | |
| person.identifier.scopus-author-id | 55644767300 | |
| project.funder.identifier | http://doi.org/10.13039/501100001871 | |
| project.funder.name | Fundação para a Ciência e a Tecnologia | |
| rcaap.rights | openAccess | pt_PT |
| rcaap.type | article | pt_PT |
| relation.isAuthorOfPublication | f3fb450f-5f22-4f0c-8916-7742d519f6af | |
| relation.isAuthorOfPublication.latestForDiscovery | f3fb450f-5f22-4f0c-8916-7742d519f6af | |
| relation.isProjectOfPublication | e9972dd7-ceaf-49ee-959a-d2a0e393b124 | |
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