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Valorization of apple tree wood residues by polyphenols extraction: Comparison between conventional and microwave-assisted extraction

dc.contributor.authorMoreira, Manuela M.
dc.contributor.authorBarroso, M. Fátima
dc.contributor.authorBoeykens, Annick
dc.contributor.authorWithouck, Hannes
dc.contributor.authorMorais, Simone
dc.contributor.authorDelerue-Matos, Cristina
dc.date.accessioned2019-04-16T13:52:25Z
dc.date.available2019-04-16T13:52:25Z
dc.date.issued2017
dc.description.abstractFor the first time, the characterization of antioxidant activity and phenolic profile of apple tree (Malus domestica) bark, core and roots was carried out. Phenolic compounds were extracted from the Belgium apple tree wood residues collected at two seasons, namely summer 2015 and winter 2016, using conventional (CE) and microwave-assisted extraction (MAE) techniques. For each extraction technique, the influence of the most important operational parameters, namely solvent composition, extraction time and temperature, on the total phenolic and flavonoid content, and antioxidant activity by the 2,2-diphenyl-1-picrylhydrazyl radical scavenging activity (DPPH-RSA) and ferric reducing activity power (FRAP) assays were optimized. The phenolic profile from the obtained extracts was also characterized by high-performance liquid chromatography with photodiode array detection (HPLC-PDA). Optimum conditions were: 20 mL ethanol:water 60:40 v/v, 20 min, 100 °C, sample weight 0.1 g for MAE and 20 mL ethanol:water 50:50 v/v, 2 h, 55 °C, sample weight 0.5 g for CE. Root extracts obtained by MAE (the most efficient technique) presented the highest phenolic (47.7 ± 0.9 mg gallic acid equivalents/g dry weight) and flavonoid (17.1 ± 0.8 mg epicatechin equivalents/g dry weight) content, and antioxidant activity (28.4 ± 2.0 mg trolox equivalents/g dry weight and 36.1 ± 2.7 mg ascorbic acid equivalents/g dry weight for DPPH-RSA and FRAP assays, respectively), followed by bark and core wood extracts. HPLC-PDA analysis revealed that phloridzin was the main contributor to the phenolic composition representing 52%–87% of the total amount of phenolic compounds quantified, while phenolic acids represents less than 10%. This study reveals the potential of apple tree wood residues valorization through the recovery of phenolic compounds for food, pharmaceutical and cosmetic applications.pt_PT
dc.description.versioninfo:eu-repo/semantics/publishedVersionpt_PT
dc.identifier.doi10.1016/j.indcrop.2017.04.038pt_PT
dc.identifier.issn0926-6690
dc.identifier.urihttp://hdl.handle.net/10400.22/13601
dc.language.isoengpt_PT
dc.relationNORTE-01-0145-FEDER-000011-311pt_PT
dc.relationPOCI/01/0145/FERDER/007265pt_PT
dc.relation.publisherversionhttps://www.sciencedirect.com/science/article/pii/S0926669017302686?via%3Dihubpt_PT
dc.subjectApple tree woodpt_PT
dc.subjectMicrowave-assisted extractionpt_PT
dc.subjectConventional extractionpt_PT
dc.subjectAntioxidant activitypt_PT
dc.subjectPhenolic compoundspt_PT
dc.subjectHPLC analysispt_PT
dc.titleValorization of apple tree wood residues by polyphenols extraction: Comparison between conventional and microwave-assisted extractionpt_PT
dc.typejournal article
dspace.entity.typePublication
oaire.awardURIinfo:eu-repo/grantAgreement/FCT/5876/UID%2FQUI%2F50006%2F2013/PT
oaire.citation.endPage220pt_PT
oaire.citation.startPage210pt_PT
oaire.citation.titleIndustrial Crops and Productspt_PT
oaire.citation.volume104pt_PT
oaire.fundingStream5876
person.familyNamede Sá Barroso
person.familyNameMorais
person.familyNameDelerue-Matos
person.givenNameMaria de Fátima
person.givenNameSimone
person.givenNameCristina
person.identifier1598822
person.identifier.ciencia-idAF16-22E5-5EBD
person.identifier.ciencia-idB111-BBFB-F200
person.identifier.ciencia-id9A1A-43FB-5C27
person.identifier.orcid0000-0001-9011-5992
person.identifier.orcid0000-0001-6433-5801
person.identifier.orcid0000-0002-3924-776X
person.identifier.ridD-4990-2013
person.identifier.scopus-author-id25631648000
person.identifier.scopus-author-id7007053747
person.identifier.scopus-author-id6603741848
project.funder.identifierhttp://doi.org/10.13039/501100001871
project.funder.nameFundação para a Ciência e a Tecnologia
rcaap.rightsopenAccesspt_PT
rcaap.typearticlept_PT
relation.isAuthorOfPublication3d701c85-4580-4614-be6d-5a1abc8cf729
relation.isAuthorOfPublication7a9c7d63-a6c7-4159-b12d-b049b8c5c8f9
relation.isAuthorOfPublication09f6a7bd-2f15-42b0-adc5-04bd22210519
relation.isAuthorOfPublication.latestForDiscovery3d701c85-4580-4614-be6d-5a1abc8cf729
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