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A multiresidue method for the analysis of carbamate and urea pesticides from soils by microwave-assisted extraction and liquid chromatography with photodiode array detection

2008Journal article Open access
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dc.contributor.authorPaíga, Paula
dc.contributor.authorMorais, Simone
dc.contributor.authorCorreia, Manuela
dc.contributor.authorAlves, Arminda
dc.contributor.authorDelerue-Matos, Cristina
dc.date.accessioned2013-11-25T15:44:25Z
dc.date.available2013-11-25T15:44:25Z
dc.date.issued2008
dc.description.abstractA multiresidue approach using microwave-assisted extraction and liquid chromatography with photodiode array detection was investigated for the determination of butylate, carbaryl, carbofuran, chlorpropham, ethiofencarb, linuron,metobromuron, and monolinuron in soils. The critical parameters of the developed methodology were studied. Method validation was performed by analyzing freshly and aged spiked soil samples. The recoveries and relative standard deviations reached using the optimized conditions were between 77.0 ± 0.46% and 120 ± 2.9% except for ethiofencarb (46.4 ± 4.4% to 105 ± 1.6%) and butylate (22.1 ± 7.6% to 49.2 ± 11%). Soil samples from five locations of Portugal were analysed.por
dc.identifier.doi10.1080/00032710802162392pt_PT
dc.identifier.issn0003-2719
dc.identifier.issn1532-236X
dc.identifier.urihttp://hdl.handle.net/10400.22/2949
dc.language.isoengpor
dc.peerreviewedyespor
dc.publisherTaylor & Francispor
dc.relation.ispartofseriesAnalytical Letters; Vol. 41, Issue 10
dc.relation.publisherversionhttp://www.tandfonline.com/doi/abs/10.1080/00032710802162392#.UooGa39qyZQpor
dc.subjectCarbamatespor
dc.subjectLiquid chromatographypor
dc.subjectMicrowave-assisted extractionpor
dc.subjectPesticidespor
dc.subjectSoilspor
dc.subjectUreaspor
dc.titleA multiresidue method for the analysis of carbamate and urea pesticides from soils by microwave-assisted extraction and liquid chromatography with photodiode array detectionpor
dc.typejournal article
dspace.entity.typePublication
oaire.citation.endPage1772por
oaire.citation.startPage1751por
person.familyNamePaíga
person.familyNameMorais
person.familyNameDelerue-Matos
person.givenNamePaula
person.givenNameSimone
person.givenNameCristina
person.identifier1668889
person.identifier1598822
person.identifier.ciencia-id331A-5D6A-D3C8
person.identifier.ciencia-idB111-BBFB-F200
person.identifier.ciencia-id9A1A-43FB-5C27
person.identifier.orcid0000-0002-9593-1355
person.identifier.orcid0000-0001-6433-5801
person.identifier.orcid0000-0002-3924-776X
person.identifier.ridQ-4930-2018
person.identifier.ridD-4990-2013
person.identifier.scopus-author-id6506638953
person.identifier.scopus-author-id7007053747
person.identifier.scopus-author-id6603741848
rcaap.rightsopenAccesspor
rcaap.typearticlepor
relation.isAuthorOfPublication4a0677dc-0b54-4831-aa9a-4a73f0df911d
relation.isAuthorOfPublication7a9c7d63-a6c7-4159-b12d-b049b8c5c8f9
relation.isAuthorOfPublication09f6a7bd-2f15-42b0-adc5-04bd22210519
relation.isAuthorOfPublication.latestForDiscovery4a0677dc-0b54-4831-aa9a-4a73f0df911d

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